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A simple, sensitive and accurate method has been developed for the simultaneous determination of alprazolam and its major metabolite in plasma by the combination of high-performance liquid chromatography (HPLC) with a UV detector and a glassy carbon electrode (GC-ED). The separation was performed on a Tracer Extrasil ODS C18 column (250 x 4.6 mm I.D.) with a mobile phase consisting of methanol-water (25:75, v/v), and the total run time was 15 min. UV and electrochemical detection was employed at lambda = 227 nm and lambda = 310 mV, respectively. The lower limit of detection and limit of quantitation were 20 ng/mL and 50 ng/mL, respectively. The method was found to be linear in the therapeutic range of 50-400 ng/mL plasma. The relative standard deviations (%RSD) for intra- and inter-day analysis were 6.4-14.2% and 8.0-12.4%, respectively. The method was applied to a pharmacokinetic study of a single 100 mg dose of alprazolam in a healthy male rat.Albania at the 1998 Winter Olympics

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